3′,6′-Bis(ethyl­amino)-2′,7′-dimethyl-2-{[2-[(E)-3,4-methyl­enedioxy­benzyl­idene­amino]eth­yl}spiro­[isoindoline-1,9′-xanthen]-3-one

نویسندگان

  • Zhi-Hong Xu
  • Hong-Sheng Wang
  • Lian-Ting Tao
  • Hong-Wei Wang
چکیده

The title compound, C(36)H(36)N(4)O(4), was prepared as a spiro-lactam ring formation of the rhodamine dye for comparison with a ring-opened form. The xanthene ring system is approximately planar [r.m.s. deviations from planarity = 0.023 (9) Å for the xanthene ring]. The dihedral angles formed by the spiro-lactam and 1,3-benzodioxole rings with the xanthene ring system are 86.8 (1) and 74.3 (1)°, respectively.

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3′,6′-Bis(ethyl­amino)-2′,7′-dimethyl-2-{2-(E)-[(thio­phen-2-yl)methyl­idene­amino]­eth­yl}spiro­[isoindoline-1,9′-xanthen]-3-one methanol monosolvate

The title compound, C(33)H(34)N(4)O(2)S·CH(3)OH, was prepared as a spiro-lactam ring formation of rhodamine 6 G dye for comparison with a ring-opened form. The xanthene and spiro-lactam rings are approximately planar [r.m.s. deviations from planarity = 0.122 (3) and 0.072 (6) Å, respectively]. The dihedral angles formed by the spiro-lactam and thio-phene rings with the xanthene ring system are ...

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[(2-{[3′,6′-Bis(ethyl­amino)-2′,7′-dimethyl-3-oxospiro­[1H-isoindole-1,9′-9H-xanthen]-2-yl}eth­yl)amino­meth­yl]phenol. Corrigendum

The title and the chemical diagram of the paper by Zhang, Peng, Gao & Fan [Acta Cryst. (2008), E64, o403] are corrected.[This corrects the article DOI: 10.1107/S1600536807055559.].

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3′,6′-Bis(diethyl­amino)-2-[(E)-2-(4-hy­droxy-3-meth­oxy­benzyl­idene­amino)­eth­yl]spiro­[isoindoline-1,9′-xanthen]-3-one ethanol monosolvate

In the title compound, C(38)H(42)N(4)O(4)·C(2)H(6)O, prepared via a spiro-lactam ring-formation reaction in a rhodamine dye, the xanthene ring system is approximately planar (r.m.s. deviation = 0.0014Å) and subtends dihedral angles of 88.10 (3) and 86.92 (4)° with the spiro-lactam (r.m.s. deviations = 0.0012 Å) and benzene rings, respectively. The crystal structure consists of chains parallel t...

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3′,6′-Bis(ethyl­amino)-2-[(2-hydroxy­ethyl)­amino]-2′,7′-dimethylspiro­[isoindoline-1,9′-xanthen]-3-one

In the title compound, C(28)H(32)N(4)O(3), the dihedral angle between the planes of the xanthene ring system and the spiro-lactam ring is 85.99 (3)°. Mol-ecules are linked by inter-molecular O-H⋯O and N-H⋯O hydrogen-bonding inter-actions.

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3′,6′-Bis(diethyl­amino)-2-(2-hydroxy­ethyl­amino)spiro­[isoindoline-1,9′-xanthen]-3-one

In the title mol-ecule, C(30)H(36)N(4)O(3), the dihedral angle between the planes of the xanthene and spiro-lactam rings systems is 88.69 (4)°. Both C atoms of one of the ethyl groups are disordered over two sites with occupancies 0.72 (2)/0.28 (2). The conformation of the mol-ecule may be influenced by two intra-molecular hydrogen bonds.

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عنوان ژورنال:

دوره 65  شماره 

صفحات  -

تاریخ انتشار 2009